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Single crystals of T-BTD and TMS-T-BTD were grown from solutions, with the largest sizes being 7 × 2 × 0.5 mm 3 and 8 × 1 × 0.45 mm 3, respectively. Using single-crystal X-ray diffraction at 293 K, the crystal structure of T-BTD was refined in the rhombic system (sp.gr. P cab , Z = 8), while for TMS-T-BTD, it was determined for the first time in the monoclinic system (sp.gr. P2 1 /c, Z = 4).
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